Crystal structure of (2-(2-chlorophenyl)-5-ethyl-1,3-dioxan-5-yl)methanol hemihydrate, C13H17ClO3 · 0.5 H2O
نویسندگان
چکیده
منابع مشابه
Crystal structure of ethyl 2-(4-chlorophenyl)-3-cyclopentyl-4-oxo-1-propylimidazolidine-5-carboxylate
The title compound, C20H27ClN2O3, was obtained via an original synthesis method. The central heterocyclic ring adopts a shallow envelope conformation, with the N atom bearing the cyclo-pentane ring as the flap [deviation from the other atoms = 0.442 (2) Å]. The cyclo-pentane ring adopts a twisted conformation about one of the CN-C bonds: the exocyclic C-N bond adopts an equatorial orientation. ...
متن کاملCrystal structure of 1-ethyl-5-iodoindolin-2-one
In the title indolinone derivative, C10H10INO, all the non-H atoms, except the terminal methyl C atom, are almost coplanar. The mol-ecules are arranged into columns extending along the a-axis direction and inter-act with the mol-ecules in adjacent columns via C-H⋯O hydrogen bonds [H⋯O distance = 2.57 (3) Å] and I⋯I short contacts of 3.8986 (3) Å. A one-dimensional zigzag iodine chain along the ...
متن کامل2-(2-Nitrophenyl)-1,3-dioxan-5-ol
In the title compound, C(10)H(11)NO(5), the six-membered 1,3-dioxane ring displays a chair conformation, with the hydr-oxy and 2-nitro-phenyl groups in equatorial positions, which minimizes steric hindrance. In the crystal, mol-ecules are linked into chains along the b axis by inter-molecular O-H⋯O hydrogen bonds.
متن کاملCrystal structure of 2-[(5',6',7',8'-tetrahydro-5',5',8',8'-tetramethyl)-2'-naphthyl]-1-ethyl-1H-benzimidazole-5-carboxylic acid ethyl ester.
retinoids with a tetrahydronaphthalene structure (Fig. 1), was synthesized using an NaHSO3 addition product of 5,6,7,8tetrahydro-5,5,8,8-tetramethyl-2-naphthalene-carboxaldehyde (compound I) as a starting material, which was prepared as described.1 The condensation of compound I and 4-ethylamino3-amino-ethylbenzoate (mp: 73 ̊C) in DMF for 70 h gave the title compound (recrystallized from hexane/...
متن کامل(2-tert-Butyl-5-hydroxymethyl-1,3-dioxan-5-yl)methanol
In the title compound, C(10)H(20)O(4), the dioxane ring adopts a chair conformation. The tert-butyl group occupies an equatorial position, and is staggered with respect to the O atoms of the dioxane ring. In the crystal, mol-ecules are connected by O-H⋯O hydrogen-bonds into zigzag chains of R(4) (4)(8) and R(2) (2)(12) ring motifs that run parallel to the a axis.
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Zeitschrift für Kristallographie - New Crystal Structures
سال: 2016
ISSN: 2197-4578,1433-7266
DOI: 10.1515/ncrs-2015-0109